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EAVF General Assembly, Pavia (Italy) | 20 October 2023
Volume 14 - 2023 | https://doi.org/10.3389/fpls.2023.1260431
This article is part of the Research TopicPlant-Based Solutions for Ecosystem Quality Assessment and Remediation StrategiesView all 7 articles
Mercury (Hg) is a global environmental concern due to its toxicity (especially high in methylated form) and the long-range distribution of its gaseous elemental form (GEM)
pose intrinsic difficulties for their management and heavy monitoring costs
plant-based solutions may play a key role in the ecosystem quality assessment and support remediation strategies
combining reliability and cost-effectiveness
we adopted a biomonitoring approach by using tree rings of four different species collected in the proximity of the mining-metallurgical area of Abbadia San Salvatore
a major former Hg mining district whose reclamation is currently in progress
Our dendrochemical analysis was aimed at identifying the historical changes of local atmospheric Hg contamination and at singling out
other potentially toxic elements (PTEs) associated with the past mining activity
Collected cores dated back to early as 1940 and provided the temporal patterns of atmospheric Hg emission vs the produced liquid quantities
so reconstructing the historical impact of the mining site on nearby terrestrial ecosystems and resident human population
Current GEM contamination was found about twenty times lower than that of the fully operational mine periods
thallium (Tl) and lead (Pb) appeared to be potentially associated with the mining activity
thus suggesting new working assumptions for further dendrochemical analyses and for the inclusion of Pb in human biomonitoring surveys of the Mt
The results prompt a more thorough assessment by tracking for a longer time span a critical site that is an ideal open-field lab to study the ecophysiology of different tree species in relation to environmental behavior of PTEs for better-assessing wildlife and human exposures
Through analysis of tree rings from four different species
we aimed to identify the temporal patterns of atmospheric Hg emission vs the produced quantities to reconstruct the historical impact of the mining site on nearby terrestrial ecosystems and resident population
In a first attempt to single out possible tracers of local elemental contamination
other potentially toxic elements (PTEs) that could be associated with the mining-metallurgical activities in Abbadia S.S
GEM concentrations map of the mining site of Abbadia S.S. and the nearby urban area, recently produced by using passive samplers (McLagan et al., 2019), was taken in this study as the main reference for sampling design. Sampling sites (Figure 1) were selected considering GEM dispersal from the metallurgical plant, the hotspot of contamination in the area (McLagan et al., 2019)
the selected sampling sites were at a distance of 340-500 m in zones where it was possible to locate trees of four species: maple (Acer pseudoplatanus)
chestnut (Castanaea sativa) and linden (Tilia cordata)
Figure 1 Sampling sites of tree cores in the area of the Mine of Abbadia San Salvatore (Google Earth) and superimposed representation of the distribution of time-weighted average concentrations of GEM as reported by McLagan et al., 2019
Tree cores were collected in October 2022 using a 400 mm long Haglöf increment borer
Two cores from each tree were taken from the east and west sides of the trunk
cleaning actions were put in place to avoid any potential contamination (e.g
and the borer was washed with Milli-Q water and blown drying with canned air prior to use and after each sampling)
each core was stored in a 600 mm long 10 mm diameter PVC pipe which was sealed with a rubber socket cap on each end
samples were stored in a freezer at -20°C and later dried at room temperature for a week
After cross-dating the cores with standard dendrochronological methods
ring widths were measured with a dissecting Leica microscope; starting from the outside towards the center
the cores were finally cut into 3-year segments for linden and into 5-year segments for the other species (3-year the innermost chestnut segment) and lyophilized in a LIO 5Pascal (t = 24 h
P = 0,125 mbar) prior to analysis to achieve complete dryness
Total concentrations of Hg and 13 other elements
vanadium (V) and zinc (Zn) of each core segment were determined at the Core Facility - CFH of the University of Hohenheim by using an inductively coupled plasma mass spectrometer (ICP-MS
PerkinElmer) after mineralization with HNO3 and H2O2 in a microwave digestion unit (UltraCLAVEIII
samples and rinse solution to prevent the memory effects of Hg
rhodium ICP standard solution as internal standards together with certified reference materials (1547 “Peach Leaves” and 1573a “Tomato Leaves” from NIST
USA and n° 62 “Olive Leaves” from BCR
Results of each batch of 24 samples were accepted only if data obtained from the certified reference materials were within the uncertainty range of the certified values (intervals with 95% confidence)
Analytical precision from 6 replicate of certified reference materials
subjected to the same procedure as the wood samples
Concentrations of elements were expressed as mg/kg on a dry weight basis
Collected tree cores dated back to as early as the year 1942 for linden, 1960 for chestnut, and 1978 for pine and maple. In Table 1 the overall concentrations of Hg and the other trace elements determined in tree ring core segments were reported
Cd and Co were very low in tree rings from Abbadia S.S.
with median concentrations of 0.03 – 0.04 mg/kg or below the DL
Tl concentrations were generally negligible except for linden and maple cores
which showed concentrations up to 0.14-0.15 mg/kg
Overall Hg concentrations in core segments of tree species were considerable as they varied from the DL (0.05 mg/kg) up to the maximum level of 3.37 mg/kg found in the linden tree core
Table 1 Mercury and PTEs concentrations (median
min-max; mg/kg) in tree rings from stands of four species (A
n=27) collected from the urban area of Abbadia S.S
Figure 2 Projections of concentration data from tree ring segments in the vector space defined by PCA
Figure 3 Total Hg concentrations in core segments collected from the linden tree (3-years segments) and from chestnut and pine trees (5-years segments) compared with the trend of liquid Hg tons produced in the mining district of Mt. Amiata (years 1942-2022); Hg produced quantities (Segreto, 1991; Forconi, 2011) were averaged for the corresponding time intervals of the segments
Keeping in mind the limitations of our pilot study
we can speculate about the possibility to include Pb in the parameter list of the next human biomonitoring campaigns
despite significant gaps in the knowledge of the ecophysiological mechanisms driving the PTEs cycling in trees and their transport and accumulation in woody tissues
tree ring analysis is a promising tool to infer past and present impacts on environmental quality and to evaluate the resulting human exposure
The raw data supporting the conclusions of this article will be made available by the authors
The author(s) declare financial support was received for the research
The author(s) declare that financial support has been received from the University of Siena for the publication of this article
The authors declare that the research was conducted in the absence of any commercial or financial relationships that could be construed as a potential conflict of interest
All claims expressed in this article are solely those of the authors and do not necessarily represent those of their affiliated organizations
Any product that may be evaluated in this article
or claim that may be made by its manufacturer
is not guaranteed or endorsed by the publisher
Historical smelting activities in Eastern Canada revealed by Pb concentrations and isotope ratios in tree rings of long-lived white cedars (Thuja occidentalis L.)
Evaluation of historical atmospheric pollution in an industrial area by dendrochemical approaches
doi: 10.1016/j.chemosphere.2018.12.072
Spatiotemporal reconstruction of lead contamination using tree rings and organic soil layers
and when of dendrochemistry: (paleo) environmental information from the chemical analysis of tree rings
Ecological study of the mercury-bearing area of Monte Amiata
Mortality of populations residing in geothermal areas of Tuscany during the period 2003-2012
400-year record of atmospheric mercury from tree-rings in Northwestern Canada
Il cinabro sul Monte Amiata (Abbadia San Salvatore
Google Scholar
Tree rings record of long-term atmospheric hg pollution in the monte amiata mining district (Central Italy): lessons from the past for a better future
Tree rings as historical archives of atmospheric mercury: A critical review
Further investigations into the use of tree rings as archives of atmospheric mercury concentrations
CrossRef Full Text | Google Scholar
Internal tree cycling and atmospheric archiving of mercury: examination with concentration and stable isotope analyses
Characterization and quantification of atmospheric mercury sources using passive air samplers
Mihaljevič
Lead isotopic and metallic pollution record in tree rings from the copperbelt mining-smelting area
Air quality in post-mining towns: tracking potentially toxic elements using tree leaves
Lichen transplants as indicators of gaseous elemental mercury concentrations
Levels and determinants of urinary and blood metals in the geothermal area of Mt
Investigation of spatial and historical variations of air pollution around an industrial region using trace and macro elements in tree components
Mercury accumulation in leaves of different plant types - the significance of tissue age and specific leaf area
Health effects among a cohort exposed to low-level arsenic in a geothermal area of Tuscany
Influence of ore processing activity on Hg
As and Sb contamination and fractionation in soils in a former mining site of Monte Amiata ore district (Italy)
doi: 10.1016/j.chemosphere.2018.02.051
exploitation and environmental impact of the Mt
Amiata mercury ore district (Southern Tuscany
Strategie internazionali e vincoli extraeconomici (Milano
Google Scholar
Distribution of thallium and accompanying metals in tree rings of Scots pine (Pinus sylvestris L.) from a smelter-affected area
Thallium and potentially toxic elements distribution in pine needles
tree rings and soils around a pyrite mine and indication for environmental pollution
Application of tree rings [dendrochemistry] for detecting historical trends in air Hg concentrations across multiple scales
Trace element transformations and partitioning during the roasting of pyrite ores in the sulfuric acid industry
PubMed Abstract | CrossRef Full Text | Google Scholar
Mercury uptake by vegetation and impacts on global mercury cycling
CrossRef Full Text | Google Scholar
Loppi S and Monaci F (2023) Tree-rings analysis to reconstruct atmospheric mercury contamination at a historical mining site
Received: 17 July 2023; Accepted: 27 September 2023;Published: 13 October 2023
Copyright © 2023 Baroni, Ancora, Franzaring, Loppi and Monaci. This is an open-access article distributed under the terms of the Creative Commons Attribution License (CC BY)
distribution or reproduction in other forums is permitted
provided the original author(s) and the copyright owner(s) are credited and that the original publication in this journal is cited
in accordance with accepted academic practice
distribution or reproduction is permitted which does not comply with these terms
*Correspondence: Fabrizio Monaci, ZmFicml6aW8ubW9uYWNpQHVuaXNpLml0
Disclaimer: All claims expressed in this article are solely those of the authors and do not necessarily represent those of their affiliated organizations
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Medievalists.net
A new DNA study shows that 14th century plague outbreaks might have resulted from repeated introductions of Yersinia pestis to Europe
would have contributed to the rapid spread of the Black Death and other epidemics throughout Europe
The bacterium Yersinia pestis is the causative agent of bubonic and pulmonary plague in humans
Plague is primarily a disease of wildlife and is maintained in reservoirs
which nowadays are present on all continents with the exception of Australia and Western Europe
represents one of the most significant events that marked the beginning of the second plague pandemic during the medieval period
plague spread through whole Europe like wildfire
leading to the decline of the European population by 30 %
After this dramatic period and for more than 350 years
Europe knew a series of recurrent devastating outbreaks of Y
different studies tried to understand the origin of these outbreaks
after a first introduction during the Black Death
pestis were established in Western Europe – which explains these recurrent outbreaks
“The other hypothesis suggest that the plague was repeatedly introduced to Western Europe from a reservoir located in Eastern Europe/Central Asia and spread via commercial trade routes and human movement”
these two scenarios are investigated using five newly presented ancient genomes (aDNA) of Y
pestis isolated from skeletons distributed in archaeological sites from South (Abbadia San Salvatore
France) to North Europe (Bergen-op-Zoom in the Netherlands and Oslo
The ancient genomes from Abbadia San Salvatore and Oslo are the first ancient DNA sequences reported from Italy and Norway
Historical data investigation of contacts and bed testaments conducted by the authors revealed the high percentage of people killed by plague within four months from late June to early September 1348 in Abbadia San Salvatore
Centre for Ecological and Evolutionary Synthesis researcher Amine Namouchi and colleagues advance in their paper that these two additional point mutations were acquired through a large transmission chain in Italy
rather than having been gained within a newly established local wildlife reservoir
the authors found that it is most likely dated to 1348
archeological and radiocarbon dating data described in their paper
While the origin of the Black Death remains unclear
the authors advance a new hypothesis that relates the onset of the Black Death with the arrival of a considerable variety of fur in the ports of the Black Sea by 1340 from trade routes starting from Sarai
during the same period a new mainland route connecting Sarai
Tana and Caffa had been established with the support of the Golden Horde
The Golden Horde was originally a Mongol and later Turkicized khanate established in the 13th century and originating as the northwestern sector of the Mongol Empire
The Crimean Khanate and the Kazakh Khanate
the authors confirm the so-called pestis secunda that occured from 1357 to 1366
“The group of aDNA that belongs to thepestis secundaincludes samples from London
Bolgar-City (Russia) and the newly presented two aDNA from Bergen-op-Zoom
Four point mutations separate the group of aDNA of the Black Death from the group that belongs to thepestis secunda
we claim that thepestis secundamight also be the result of the introduction ofY
pestisalong the fur trade routes established between Novgorod (Russia) and Western Europe through the Hanseatic League”
by describing all previously and newly described aDNA of Y
Namouchi and colleagues provided additional evidence that the recurrent plague outbreaks during the Second plague Pandemic were the result of multiple waves of introduction of Y
pestis from a reservoir located in Eastern Europe/Central Asia
This result is in line with previous studies based on ecological evidence
as-well-as human movement would have contributed to the rapid spread of plague throughout Europe during the Middle Ages
Click here to read the article “Integrative approach using Yersinia pestisgenomes to revisit the historical landscape of plague during the Medieval Period” from PNAS
Top Image: The fur trade from the East towards Western Europa followed two major routes during the Middle Ages
Illustration courtesy Amine Namouchi / University of Oslo
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